1-Bromotetradecane cas 112-71-0

Products Name

1-Bromotetradecane

1-Bromotetradecane Details
Chemical Name: 1-Bromotetradecane

CAS No.: 112-71-0

Molecular Formula: C14H29Br

Molecular weight: 277.28
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1-Bromotetradecane Typical Properties

 Item
 Method of Analysis
 Standard
 Result

 appearance
 visual inspection
 Colorless transparent liquid
 Colorless transparent liquid

 Purity
 gas chromatography
 ≥99.0%
 99.36%

 moisture
 –
 <0.05%

0.038%

1-Bromotetradecane Usage
Used in organic synthesis, can be used in the synthesis of medicine and other fine chemicals.
production method
Derived from tetradecanol by bromination.

Add myristyl alcohol to the reaction pot, add sulfuric acid dropwise with stirring, and continue stirring for half an hour after the addition.
Then add hydrobromic acid, heat to 99-101 ℃, and react for 8h. Cool to 30 ° C, stop stirring, leave for 12h, separate the upper oily substance, and adjust the pH to 8 with 10% sodium carbonate solution.
Separate the water layer, and wash the oil twice with an equal volume of 50% ethanol. Add the washed oil to sodium carbonate, stir intermittently, and dry for 24 hours. Filter to get the finished product.

1-Bromotetradecane Packing
 25kgs/drum
1-Bromotetradecane Storage
 1-Bromotetradecane should be stored in a closed system, and be kept in a dry dark place without any light exposure. The shelf life is two years in original, unopened containers.

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